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iyas (iyas)
Junior Member
Username: iyas

Post Number: 8
Registered: 7-2007
Posted on Tuesday, February 12, 2008 - 11:48 am:   

i am still working on building the method
there are too many difficulties ,
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venkatarman (venkynir)
Senior Member
Username: venkynir

Post Number: 54
Registered: 3-2004
Posted on Tuesday, February 12, 2008 - 5:38 am:   

Mr. Iyas ;
Fine. Tell me you are interset granualtion alone or with granualtion with LOD you want work in line process variables?
can you share your same data with us for suggestion and method building ?
The sample is set depends upon the range and closness your are going to measure .
Thumb role more samples closer to true value and robust model can build up
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venkatarman (venkynir)
Senior Member
Username: venkynir

Post Number: 53
Registered: 3-2004
Posted on Tuesday, February 12, 2008 - 5:35 am:   

Mr. Iyas ;
Fine tell me you are interset granualtion alone or with granualtion with LOD you want work in line process variables?
can you share your same data with us for suggestion and method building ?
The sample is set depends upon the range and closness your are going to measure .
Thumb role more samples closer to true value and robust model can build.
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iyas (iyas)
Junior Member
Username: iyas

Post Number: 7
Registered: 7-2007
Posted on Monday, February 11, 2008 - 11:12 pm:   

if you please can you guide me about this subject
Using NIR (Near Infrared ) in homogeneity test for bulk products of vitamins B1,B6 B12 prepared for granulation as indicator of process validation
is it applicable ?
is 60-100 sample set is enough ?
can be done by the NIR and how to set up the experiment
sorry for my too many questions
waiting for your answer

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